写论文之TPR方法描述（1）

描述我们用了TPR技术
The reduction behaviors and the interactions between the active phase and the support of each sample were examined by using temperature-programmed reduction of H2 (H2-TPR) technique.

写样品怎么放置
Each sample was placed in a quartz tubular reactor fitted with a thermocouple for continuous temperature measurement.

写测试之前我们对管道进行净化
Prior to the H2-TPR measurement, to drive away water or impurities, 5% Co/Al2O3 catalyst (0.6 g) were flushed with high purity argon at 200 °C for 1 h, respectively.

描述我们开始测试了。
10% H2/Ar was switched on and the flow rate through the reactor was controlled at 30 mL/min.

The temperature was raised at a rate of 6 °C/min from 25 to 750 °C or at a rate of 10 °C/min from 25 to 950 °C and was held at the final temperature for 10 min.

描述我们如何记录信号
The H2 consumption (TCD signal) was recorded automatically by a PC.

参考
Comparative Study on the Formation and Reduction ...